C₂₆H₁₉N

Base Information

• Chemical Name: C₂₆H₁₉N
• CAS No.: 1402905-43-4
• Molecular Formula: C₂₆H₁₉N
• Molecular Weight: 345.444
• Mol file: 1402905-43-4.mol

Synonyms:C₂₆H₁₉N

Chemical Property of C₂₆H₁₉N

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₆H₁₉N

There total 2 articles about C₂₆H₁₉N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H20ClN (1402905-62-7) → C26H19N (1402905-42-3) + C26H19N (1402905-43-4) + 6-(4'-methyl-[1,1'-biphenyl]-4-yl)phenanthridine (1402905-44-5)

Guidance literature:

With potassium tert-butylate; ethylene glycol; In toluene; at 120 ℃; for 18h; Overall yield = 77 %; Inert atmosphere; Schlenk technique;

DOI:10.1021/ol302489n DOI:10.1021/ol302489n

Reference yield:

4-benzoyl-4'-methylbiphenyl (63283-56-7) + o-chloroaniline (95-51-2) → C26H19N (1402905-42-3) + C26H19N (1402905-43-4) + 6-(4'-methyl-[1,1'-biphenyl]-4-yl)phenanthridine (1402905-44-5)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc(II) chloride / toluene / Reflux; Schlenk technique

2: potassium tert-butylate; ethylene glycol / toluene / 18 h / 120 °C / Inert atmosphere; Schlenk technique

With potassium tert-butylate; ethylene glycol; zinc(II) chloride; In toluene;

DOI:10.1021/ol302489n DOI:10.1021/ol302489n

upstream raw materials:

C₂₆H₂₀ClN

4-benzoyl-4'-methylbiphenyl

o-chloroaniline