(E)-N-(1-bromo-2-methyl-4-phenylbut-3-en-2-yl)-2,2,2-trichloroacetamide

Base Information

Chemical Name:(E)-N-(1-bromo-2-methyl-4-phenylbut-3-en-2-yl)-2,2,2-trichloroacetamide
CAS No.:1620206-47-4
Molecular Formula:C₁₃H₁₃BrCl₃NO
Molecular Weight:385.515
Hs Code.:

Synonyms:(E)-N-(1-bromo-2-methyl-4-phenylbut-3-en-2-yl)-2,2,2-trichloroacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(1-bromo-2-methyl-4-phenylbut-3-en-2-yl)-2,2,2-trichloroacetamide

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Technology Process of (E)-N-(1-bromo-2-methyl-4-phenylbut-3-en-2-yl)-2,2,2-trichloroacetamide

There total 2 articles about (E)-N-(1-bromo-2-methyl-4-phenylbut-3-en-2-yl)-2,2,2-trichloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1620206-29-2
C₁₃H₁₄Cl₃NO

: 1620206-47-4
(E)-N-(1-bromo-2-methyl-4-phenylbut-3-en-2-yl)-2,2,2-trichloroacetamide

Guidance literature:: With N-bromoacetamide; In N,N-dimethyl-formamide; at 90 ℃; for 10h;
DOI:10.1039/c4ob01126k

Reference yield:

: 23092-23-1
3-methyl-1-phenylbut-3-en-1-ol

: 1620206-47-4
(E)-N-(1-bromo-2-methyl-4-phenylbut-3-en-2-yl)-2,2,2-trichloroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C

2: N-bromoacetamide / N,N-dimethyl-formamide / 10 h / 90 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; N-bromoacetamide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4ob01126k