3-Methyl-1-phenyl-3-buten-1-ol

Base Information

• Chemical Name: 3-Methyl-1-phenyl-3-buten-1-ol
• CAS No.: 23092-23-1
• Molecular Formula: C11H14O
• Molecular Weight: 162.232
• DSSTox Substance ID: DTXSID901273089
• Nikkaji Number: J305.747J
• Mol file: 23092-23-1.mol

Synonyms:3-methyl-1-phenylbut-3-en-1-ol;1-phenyl-3-methyl-3-buten-1-ol;3-methyl-1-phenyl-3-buten-1-ol;23092-23-1;SCHEMBL3241455;MZMDMSHZBSFWOL-UHFFFAOYSA-N;DTXSID901273089;AKOS017731618;alpha-(2-Methyl-2-propen-1-yl)benzenemethanol

Chemical Property of 3-Methyl-1-phenyl-3-buten-1-ol

Chemical Property:

• XLogP3: 2.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 162.104465066
• Heavy Atom Count: 12
• Complexity: 145

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(=C)CC(C1=CC=CC=C1)O

Technology Process of 3-Methyl-1-phenyl-3-buten-1-ol

There total 92 articles about 3-Methyl-1-phenyl-3-buten-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-methylallyltributyltin (67883-62-9) + benzaldehyde (100-52-7) → 3-methyl-1-phenylbut-3-en-1-ol (23092-23-1)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 50 ℃; for 24h;

DOI:10.1021/ja9608858

Reference yield: 100.0%

2-methylallylmagnesium chloride (5674-01-1) + benzaldehyde (100-52-7) → 3-methyl-1-phenylbut-3-en-1-ol (23092-23-1)

Guidance literature:

In tetrahydrofuran;

DOI:10.1021/ol1018757

Reference yield: 99.0%

2-methallyltrimethylsilane (18292-38-1) + benzaldehyde (100-52-7) → 3-methyl-1-phenylbut-3-en-1-ol (23092-23-1)

Guidance literature:

scandium tris(trifluoromethanesulfonate); In various solvent(s); at 20 ℃; for 12h;

DOI:10.1002/1522-2675(200210)85:10<3185::AID-HLCA3185>3.0.CO;2-B

upstream raw materials:

2-methyl-3-bromo-1-propene

benzaldehyde

isobutene

isopropenyllithium

Downstream raw materials:

C₂₁H₃₀OSi₂

2-(5-Methyl-3-phenyl-4,5-dihydro-isoxazol-5-yl)-1-phenyl-ethanol

4-methyl-N-(3-methyl-1-phenylbut-3-enyl)benzenesulfonamide

[3-methyl-1-(prop-2-enyloxy)but-3-enyl]benzene