Technology Process of C25H27NO4S
There total 6 articles about C25H27NO4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H29NO5;
With
Lawessons reagent;
In
dichloromethane;
at 20 ℃;
With
chloranil;
In
dichloromethane;
for 24h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium methylate / methanol / 0.67 h / 0 - 25 °C
2.1: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / 5 h / 80 °C
3.1: hydrogen / ethanol / 3 h / 20 °C
4.1: Lawessons reagent / dichloromethane / 20 °C
4.2: 24 h
With
Lawessons reagent; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; hydrogen; sodium methylate;
In
methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 2 h / 15 - 20 °C
2.1: sodium methylate / methanol / 0.67 h / 0 - 25 °C
3.1: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,2-dimethoxyethane / 5 h / 80 °C
4.1: hydrogen / ethanol / 3 h / 20 °C
5.1: Lawessons reagent / dichloromethane / 20 °C
5.2: 24 h
With
Lawessons reagent; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; N-chloro-succinimide; hydrogen; sodium methylate;
In
methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;