N-p'-chlorobenzylidene-o-phenylenediamine

Base Information Edit

Chemical Name:N-p'-chlorobenzylidene-o-phenylenediamine
CAS No.:100375-14-2
Molecular Formula:C₁₃H₁₁ClN₂
Molecular Weight:230.697
Hs Code.:
Mol file:100375-14-2.mol

Synonyms:N-p'-chlorobenzylidene-o-phenylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-p'-chlorobenzylidene-o-phenylenediamine Edit

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Technology Process of N-p'-chlorobenzylidene-o-phenylenediamine

There total 3 articles about N-p'-chlorobenzylidene-o-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 104-88-1
4-chlorobenzaldehyde

: 95-54-5
1,2-diamino-benzene

: 100375-14-2
N-p'-chlorobenzylidene-o-phenylenediamine

Guidance literature:: In methanol; at 20 ℃; for 1h; Darkness;
DOI:10.1039/d0cy01164a

Reference yield: 82.0%

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 29634-58-0
N-(4-chlorobenzylidene)-2-nitroaniline

: 1019-85-8
2-(4-chlorophenyl)benzimidazole

: 100375-14-2
N-p'-chlorobenzylidene-o-phenylenediamine

: 2Ru⁽²⁺⁾*4CO*2C₁₃H₉N₂Cl^(2-)={Ru(CO)2(C₁₃H₉N₂Cl)}2

Guidance literature:: With carbon monoxide; In toluene; byproducts: CO2; High Pressure; (N2), autoclave; CO is introduced (P(CO)=50 bar), react. of Ru3(CO)12 with ClC6H4CHNC6H4NO2 at 220°C for 3.5 h under magnetic stirring; autoclave is cooled rapidly (ice bath) and then blown off, substituted benzimidazole is filtered off, Ru complex isolated by chromy. (silica gel, CH2Cl2/EtOH);
DOI:10.1016/0304-5102(92)85006-2