Se-phenyl 2-aminobenzenecarboselenoate

Base Information

• Chemical Name: Se-phenyl 2-aminobenzenecarboselenoate
• CAS No.: 1423629-95-1
• Molecular Formula: C₁₃H₁₁NOSe
• Molecular Weight: 276.196
• Mol file: 1423629-95-1.mol

Synonyms:Se-phenyl 2-aminobenzenecarboselenoate

Chemical Property of Se-phenyl 2-aminobenzenecarboselenoate

Chemical Property:

Purity/Quality:

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Technology Process of Se-phenyl 2-aminobenzenecarboselenoate

There total 1 articles about Se-phenyl 2-aminobenzenecarboselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

isatoic anhydride (118-48-9) + diphenyl diselenide (1666-13-3) → Se-phenyl 2-aminobenzenecarboselenoate (1423629-95-1)

Guidance literature:

With sodium dithionite; water; potassium carbonate; In dimethyl sulfoxide; at 60 ℃; for 1h;

DOI:10.1016/j.tet.2013.01.024

Reference yield: 94.0%

Se-phenyl 2-aminobenzenecarboselenoate (1423629-95-1) + N-benzylethylenediamine (4152-09-4) → 2-amino-N-[2-(benzylamino)ethyl]benzamide

Guidance literature:

In ethanol; at 20 ℃; for 2h; chemoselective reaction;

DOI:10.1021/acs.joc.7b00173

Reference yield: 84.0%

Se-phenyl 2-aminobenzenecarboselenoate (1423629-95-1) + 3-amino-2-propanol (78-96-6,1674-56-2) → 2-amino-N-(2-hydroxypropyl)benzamide

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 2h; chemoselective reaction;

DOI:10.1021/acs.joc.7b00173

upstream raw materials:

isatoic anhydride

diphenyl diselenide

Downstream raw materials:

2-amine-N-(methoxycarbonylmethyl)benzamide