5-Bromo-2-(2,2-diethoxyethoxy)-3-ethylbenzaldehyde

Base Information

Chemical Name:5-Bromo-2-(2,2-diethoxyethoxy)-3-ethylbenzaldehyde
CAS No.:137206-74-7
Molecular Formula:C₁₅H₂₁BrO₄
Molecular Weight:345.233
Hs Code.:
DSSTox Substance ID:DTXSID801230226

Synonyms:5-bromo-2-(2,2-diethoxyethoxy)-3-ethylbenzaldehyde;DTXSID801230226;137206-74-7

Suppliers and Price of 5-Bromo-2-(2,2-diethoxyethoxy)-3-ethylbenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Bromo-2-(2,2-diethoxyethoxy)-3-ethylbenzaldehyde

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:344.06232
Heavy Atom Count:20
Complexity:269

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC1=C(C(=CC(=C1)Br)C=O)OCC(OCC)OCC

Technology Process of 5-Bromo-2-(2,2-diethoxyethoxy)-3-ethylbenzaldehyde

There total 2 articles about 5-Bromo-2-(2,2-diethoxyethoxy)-3-ethylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 57704-12-8
5-bromo-3-ethylsalicylaldehyde

: 2032-35-1
Bromoacetaldehyde diethyl acetal

: 137206-74-7
2,2-diethoxyethyl (4-bromo-6-ethyl-2-formyl)phenyl ether

Guidance literature:: With potassium carbonate; N,N-dimethyl-formamide; for 1.5h; Heating;
DOI:10.1002/jhet.5570280535

Reference yield:

: 18980-21-7
4-bromo-2-ethylphenol

: 137206-74-7
2,2-diethoxyethyl (4-bromo-6-ethyl-2-formyl)phenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / hexamethylenetetramine, glacial acetic acid, sulfuric acid / 18 h / 25 °C

2: 80 percent / potassium carbonate, N, N-dimethylformamide / 1.5 h / Heating

With hexamethylenetetramine; sulfuric acid; potassium carbonate; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570280535