Technology Process of C42H50N2O8
There total 8 articles about C42H50N2O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C34H44N2O6;
With
sodium hydrogencarbonate;
In
1,4-dioxane;
at 0 ℃;
for 0.25h;
benzyl chloroformate;
In
1,4-dioxane; water;
for 4h;
Further stages.;
DOI:10.1021/ja077853c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium chloride; zinc / ethanol; water / 90 °C
2: sodium hydrogencarbonate / 1,4-dioxane; water / 4 h / 0 °C
With
sodium hydrogencarbonate; ammonium chloride; zinc;
In
1,4-dioxane; ethanol; water;
DOI:10.1021/jo200553g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium sulfate / dichloromethane / 4 h / 20 °C
2.1: iodine; magnesium; ethylene dibromide / tetrahydrofuran / Reflux
2.2: 5 h / -50 °C
3.1: ammonium chloride; zinc / ethanol; water / 90 °C
4.1: sodium hydrogencarbonate / 1,4-dioxane; water / 4 h / 0 °C
With
iodine; sodium hydrogencarbonate; magnesium sulfate; ammonium chloride; magnesium; ethylene dibromide; zinc;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1021/jo200553g