Technology Process of C34H41F3N8O7
There total 19 articles about C34H41F3N8O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
methanol;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: sulfuric acid / 12 h / Reflux
2: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 24 h / Reflux
3: ammonia / methanol
4: triethylamine / dichloromethane
5: water; lithium hydroxide / tetrahydrofuran; methanol
6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / tetrahydrofuran
7: N-ethyl-N,N-diisopropylamine; ammonia / isopropyl alcohol / 12 h
8: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C
9: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 20 °C
With
dmap; N-Bromosuccinimide; ammonia; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
sulfuric acid; palladium 10% on activated carbon; dibenzoyl peroxide;
In
tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / tetrahydrofuran
2: N-ethyl-N,N-diisopropylamine; ammonia / isopropyl alcohol / 12 h
3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C
4: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 20 °C
With
dmap; ammonia; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; isopropyl alcohol;