4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

Base Information

Chemical Name:4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid
CAS No.:1034343-24-2
Molecular Formula:C₁₈H₂₀O₇
Molecular Weight:348.353
Hs Code.:

Synonyms:4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

Suppliers and Price of 4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

There total 4 articles about 4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1034343-25-3
methyl 4-O-benzyl-3,5-di-O-methoxymethylgallate

: 1034343-24-2
4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; water; for 2h; Heating;
DOI:10.1021/ja803111z

Reference yield:

: 100-39-0
benzyl bromide

: 1034343-24-2
4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydrogencarbonate; potassium iodide / N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

3: lithium hydroxide; water / methanol; tetrahydrofuran / 2 h / Reflux

With water; sodium hydride; potassium hydrogencarbonate; potassium iodide; lithium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo4003135

Reference yield:

: 91925-82-5
3,5-dihydroxy-4-(phenylmethoxy)benzoic acid methyl ester

: 1034343-24-2
4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

2: lithium hydroxide; water / methanol; tetrahydrofuran / 2 h / Reflux

With water; sodium hydride; lithium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo4003135