p-nitrophenyl 2-acetamido-2,6-dideoxy-β-D-gluco-heptopyranosylurononitrile

Base Information

Chemical Name:p-nitrophenyl 2-acetamido-2,6-dideoxy-β-D-gluco-heptopyranosylurononitrile
CAS No.:890531-53-0
Molecular Formula:C₁₅H₁₇N₃O₇
Molecular Weight:351.316
Hs Code.:

Synonyms:p-nitrophenyl 2-acetamido-2,6-dideoxy-β-D-gluco-heptopyranosylurononitrile

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Chemical Property of p-nitrophenyl 2-acetamido-2,6-dideoxy-β-D-gluco-heptopyranosylurononitrile

Chemical Property:

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Technology Process of p-nitrophenyl 2-acetamido-2,6-dideoxy-β-D-gluco-heptopyranosylurononitrile

There total 6 articles about p-nitrophenyl 2-acetamido-2,6-dideoxy-β-D-gluco-heptopyranosylurononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 890531-59-6
p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile

: 890531-53-0
p-nitrophenyl 2-acetamido-2,6-dideoxy-β-D-gluco-heptopyranosylurononitrile

Guidance literature:: With water; trifluoroacetic acid; at 40 ℃; for 2h;
DOI:10.1002/ejoc.200500755

Reference yield:

: 890531-57-4
p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranoside

: 890531-53-0
p-nitrophenyl 2-acetamido-2,6-dideoxy-β-D-gluco-heptopyranosylurononitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / Ph₃P; imidazole; I₂ / toluene / 2 h / Heating

2: 43 percent / tetrahydrofuran / 16 h / 20 °C

3: 84 percent / TFA; water / 2 h / 40 °C

With 1H-imidazole; water; iodine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; toluene;
DOI:10.1002/ejoc.200500755

Reference yield:

: 890531-58-5
p-nitrophenyl 2-acetamido-2,6-dideoxy-6-iodo-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranoside

: 890531-53-0
p-nitrophenyl 2-acetamido-2,6-dideoxy-β-D-gluco-heptopyranosylurononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / tetrahydrofuran / 16 h / 20 °C

2: 84 percent / TFA; water / 2 h / 40 °C

With water; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1002/ejoc.200500755