p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile

Base Information

Chemical Name:p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile
CAS No.:890531-59-6
Molecular Formula:C₂₁H₂₇N₃O₉
Molecular Weight:465.46
Hs Code.:

Synonyms:p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile

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Chemical Property of p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile

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Technology Process of p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile

There total 5 articles about p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 890531-58-5
p-nitrophenyl 2-acetamido-2,6-dideoxy-6-iodo-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranoside

: 10442-39-4
tetra-n-butylammonium cyanide

: 890531-59-6
p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1002/ejoc.200500755

Reference yield:

: 890531-57-4
p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranoside

: 890531-59-6
p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Ph₃P; imidazole; I₂ / toluene / 2 h / Heating

2: 43 percent / tetrahydrofuran / 16 h / 20 °C

With 1H-imidazole; iodine; triphenylphosphine; In tetrahydrofuran; toluene;
DOI:10.1002/ejoc.200500755

Reference yield:

: 824-78-2
4-nitrophenol sodium salt

: 890531-59-6
p-nitrophenyl 2-acetamido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-heptopyranosylurononitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylformamide / 16 h / 20 °C

1.2: NaOMe / methanol

2.1: 79 percent / camphorsulfonic acid / methanol / 6 h / Heating

3.1: 65 percent / Ph₃P; imidazole; I₂ / toluene / 2 h / Heating

4.1: 43 percent / tetrahydrofuran / 16 h / 20 °C

With 1H-imidazole; camphor-10-sulfonic acid; iodine; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.200500755