(E)-ethyl 3-(4-(4-(chlorosulfonyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate

Base Information

• Chemical Name: (E)-ethyl 3-(4-(4-(chlorosulfonyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate
• CAS No.: 1234367-26-0
• Molecular Formula: C₁₈H₁₅ClF₂O₅S
• Molecular Weight: 416.83

Synonyms:(E)-ethyl 3-(4-(4-(chlorosulfonyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate

Chemical Property of (E)-ethyl 3-(4-(4-(chlorosulfonyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate

Chemical Property:

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Technology Process of (E)-ethyl 3-(4-(4-(chlorosulfonyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate

There total 1 articles about (E)-ethyl 3-(4-(4-(chlorosulfonyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(E)-ethyl 3-(3,5-difluoro-4-phenoxyphenyl)-2-methylacrylate (1234367-25-9) → (E)-ethyl 3-(4-(4-(chlorosulfonyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate (1234367-26-0)

Guidance literature:

With chlorosulfonic acid; In dichloromethane; for 2h; Inert atmosphere;

Reference yield:

(E)-ethyl 3-(4-(4-(chlorosulfonyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate (1234367-26-0) + (E)-ethyl 3-(4-(4-(N-(2-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)ethyl)sulfamoyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate (1234367-32-8) → N,N'-(2,2'-(2,2'-oxybis(ethane-2,1-diyl)bis(oxy))bis(ethane-2,1-diyl))bis((E)-4-(2,6-difluoro-4-(2-carbethoxypropenyl)phenoxy)benzenesulfonamide) (1234367-33-9)

Guidance literature:

With triethylamine; In dichloromethane; for 0.5h;

Reference yield:

(E)-ethyl 3-(4-(4-(chlorosulfonyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate (1234367-26-0) + 1,4-diaminobutane (110-60-1) → (E,E)-N,N'-(butane-1,4-diyl)bis(4-(2,6-difluoro-4-(2-carboethoxypropenyl)phenoxy)benzenesulfonamide) (1234367-27-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In chloroform; for 1h;

upstream raw materials:

(E)-ethyl 3-(3,5-difluoro-4-phenoxyphenyl)-2-methylacrylate

Downstream raw materials:

(E,E)-N,N'-(butane-1,4-diyl)bis(4-(2,6-difluoro-4-(2-carboethoxypropenyl)phenoxy)benzenesulfonamide)

N,N'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis((E)-4-(2,6-difluoro-4-(2-carboethoxypropenyl)phenoxy)benzenesulfonamide)

(E)-ethyl 3-(4-(4-(N-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)sulfamoyl)phenoxy)-3,5-difluorophenyl)-2-methylacrylate

N,N'-(2,2'-(2,2'-oxybis(ethane-2,1-diyl)bis(oxy))bis(ethane-2,1-diyl))bis((E)-4-(2,6-difluoro-4-(2-carbethoxypropenyl)phenoxy)benzenesulfonamide)

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