1-Benzyloxy-4-((Z)-2-methanesulfinyl-2-methylsulfanyl-vinyl)-benzene

Base Information

• Chemical Name: 1-Benzyloxy-4-((Z)-2-methanesulfinyl-2-methylsulfanyl-vinyl)-benzene
• CAS No.: 71749-20-7
• Molecular Formula: C₁₇H₁₈O₂S₂
• Molecular Weight: 318.461
• Mol file: 71749-20-7.mol

Synonyms:1-Benzyloxy-4-((Z)-2-methanesulfinyl-2-methylsulfanyl-vinyl)-benzene

Chemical Property of 1-Benzyloxy-4-((Z)-2-methanesulfinyl-2-methylsulfanyl-vinyl)-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1-Benzyloxy-4-((Z)-2-methanesulfinyl-2-methylsulfanyl-vinyl)-benzene

There total 1 articles about 1-Benzyloxy-4-((Z)-2-methanesulfinyl-2-methylsulfanyl-vinyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-benzyloxybenzaldehyde (4397-53-9) + methyl methylsulfinylmethyl sulfide (33577-16-1) → 1-Benzyloxy-4-((Z)-2-methanesulfinyl-2-methylsulfanyl-vinyl)-benzene (71749-20-7)

Guidance literature:

Multistep reaction; (i) NaOH, (ii) /BRN= 1242385/;

DOI:10.1246/bcsj.52.2013

Reference yield:

1-Benzyloxy-4-((Z)-2-methanesulfinyl-2-methylsulfanyl-vinyl)-benzene (71749-20-7) → 2-[4-(benzyloxy)benzyl]acetic acid (6547-53-1)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / 3 h / Heating

2: KOH / 1,2-dimethoxy-ethane / 19 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; In 1,2-dimethoxyethane;

DOI:10.1246/bcsj.52.2013

Reference yield:

ethanol (64-17-5) + 1-Benzyloxy-4-((Z)-2-methanesulfinyl-2-methylsulfanyl-vinyl)-benzene (71749-20-7) → 2-<4-(phenylmethoxy)phenyl>acetic acid ethyl ester (56441-69-1)

Guidance literature:

With hydrogenchloride; for 3h; Heating;

DOI:10.1246/bcsj.52.2013

upstream raw materials:

p-benzyloxybenzaldehyde

methyl methylsulfinylmethyl sulfide

Downstream raw materials:

2-<4-(phenylmethoxy)phenyl>acetic acid ethyl ester

2-[4-(benzyloxy)benzyl]acetic acid