C₆₆H₈₄N₆O₁₂S

Base Information

Chemical Name:C₆₆H₈₄N₆O₁₂S
CAS No.:271800-35-2
Molecular Formula:C₆₆H₈₄N₆O₁₂S
Molecular Weight:1185.49
Hs Code.:

C<sub>66</sub>H<sub>84</sub>N<sub>6</sub>O<sub>12</sub>S

Synonyms:C₆₆H₈₄N₆O₁₂S

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Chemical Property of C₆₆H₈₄N₆O₁₂S

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Technology Process of C₆₆H₈₄N₆O₁₂S

There total 5 articles about C₆₆H₈₄N₆O₁₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39021-83-5
3,6-dimethoxy-o-xylene

: 271800-35-2
C₆₆H₈₄N₆O₁₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: 61 percent / Nh₄NO₃; trifluoroacetic anhydride / acetonitrile / 2.5 h / 20 °C

2.1: 96 percent / H₂ / Ra-Ni / tetrahydrofuran / 18 h

3.1: SO₂NH₂ / bis-(2-methoxy-ethyl) ether / Heating

3.2: 41 percent / DMAP / 24 h / 20 °C

4.1: 100 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating

5.1: KO-t-Bu

With ammonium nitrate; N-Bromosuccinimide; potassium tert-butylate; hydrogen; SULFAMIDE; trifluoroacetic anhydride; Ra-Ni; In tetrahydrofuran; tetrachloromethane; diethylene glycol dimethyl ether; acetonitrile; 1.1: Substitution / 2.1: Catalytic hydrogenation / 3.1: Cyclization / 3.2: Acylation / 4.1: Bromination / 5.1: Substitution / 5.2: Cyclization;
DOI:10.1021/ja0005136

Reference yield:

: 186039-76-9
1,4-dimethoxy-5,6-dimethyl-2,3-dinitrobenzene

: 271800-35-2
C₆₆H₈₄N₆O₁₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: 96 percent / H₂ / Ra-Ni / tetrahydrofuran / 18 h

2.1: SO₂NH₂ / bis-(2-methoxy-ethyl) ether / Heating

2.2: 41 percent / DMAP / 24 h / 20 °C

3.1: 100 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating

4.1: KO-t-Bu

With N-Bromosuccinimide; potassium tert-butylate; hydrogen; SULFAMIDE; Ra-Ni; In tetrahydrofuran; tetrachloromethane; diethylene glycol dimethyl ether; 1.1: Catalytic hydrogenation / 2.1: Cyclization / 2.2: Acylation / 3.1: Bromination / 4.1: Substitution / 4.2: Cyclization;
DOI:10.1021/ja0005136

Reference yield:

: 186039-77-0
1,4-dimethoxy-5,6-dimethyl-2,3-diaminobenzene

: 271800-35-2
C₆₆H₈₄N₆O₁₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: SO₂NH₂ / bis-(2-methoxy-ethyl) ether / Heating

1.2: 41 percent / DMAP / 24 h / 20 °C

2.1: 100 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating

3.1: KO-t-Bu

With N-Bromosuccinimide; potassium tert-butylate; SULFAMIDE; In tetrachloromethane; diethylene glycol dimethyl ether; 1.1: Cyclization / 1.2: Acylation / 2.1: Bromination / 3.1: Substitution / 3.2: Cyclization;
DOI:10.1021/ja0005136