2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid

Base Information

Chemical Name:2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid
CAS No.:103670-02-6
Molecular Formula:C₂₉H₂₈O₁₃S
Molecular Weight:616.6
Hs Code.:

Synonyms:2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid

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Chemical Property of 2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid

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Technology Process of 2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid

There total 3 articles about 2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 54714-11-3
4,6-diphenylthieno-[3,4-d]-1,3-dioxol-2-one-5,5-dioxide

: 103670-00-4
Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronsaeure

: 103670-02-6
2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid

Guidance literature:: With pyridine; In dichloromethane; at 25 ℃; for 2h;

Reference yield:

: 103730-04-7
Brom-2,3,4-tri-O-acetyl-α-D-galactopyranosiduronsaeure

: 103670-02-6
2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / Ag₂CO₃ / methanol / 1.) 2 h, 0 deg C 2.) 24 h, 25 deg C

2: 87 percent / pyridine / CH₂Cl₂ / 2 h / 25 °C

With pyridine; silver carbonate; In methanol; dichloromethane;

Reference yield:

: 85165-61-3
Acetyl-2,3,4-tri-O-acetyl-α,β-D-galactopyranosiduronsaeure

: 103670-02-6
2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / 33percent HBr / acetic acid / 2 h / 25 °C

2: 43 percent / Ag₂CO₃ / methanol / 1.) 2 h, 0 deg C 2.) 24 h, 25 deg C

3: 87 percent / pyridine / CH₂Cl₂ / 2 h / 25 °C

With pyridine; hydrogen bromide; silver carbonate; In methanol; dichloromethane; acetic acid;