(E)-N-(Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyl)-DL-2-phenylglycin-2-(methoxycarbonyl)cinnamylester

Base Information

Chemical Name:(E)-N-(Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyl)-DL-2-phenylglycin-2-(methoxycarbonyl)cinnamylester
CAS No.:103669-77-8
Molecular Formula:C₃₂H₃₅NO₁₃
Molecular Weight:641.629
Hs Code.:

Synonyms:(E)-N-(Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyl)-DL-2-phenylglycin-2-(methoxycarbonyl)cinnamylester

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Chemical Property of (E)-N-(Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyl)-DL-2-phenylglycin-2-(methoxycarbonyl)cinnamylester

Chemical Property:

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Technology Process of (E)-N-(Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyl)-DL-2-phenylglycin-2-(methoxycarbonyl)cinnamylester

There total 6 articles about (E)-N-(Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyl)-DL-2-phenylglycin-2-(methoxycarbonyl)cinnamylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 103670-07-1
(E)-DL-2-Phenylglycin-2-(methoxycarbonyl)cinnamylester-hydrochlorid

: 103670-02-6
2,3-Dihydro-4-(methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyloxy)-3-oxo-2,5-diphenylthiophen-1,1-dioxid

: 103669-77-8
(E)-N-(Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyl)-DL-2-phenylglycin-2-(methoxycarbonyl)cinnamylester

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃;

Reference yield:

: 103669-71-2
(Z)-methyl 2-(bromomethyl)-3-phenylacrylate

: 103669-77-8
(E)-N-(Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyl)-DL-2-phenylglycin-2-(methoxycarbonyl)cinnamylester

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) HCl / 1.) THF, 15 h, reflux 2.) ether, 1 h, -30 deg C

2: 96 percent / triethylamine / CH₂Cl₂ / 25 °C

With hydrogenchloride; triethylamine; In dichloromethane;

Reference yield:

: 103670-00-4
Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronsaeure

: 103669-77-8
(E)-N-(Methyl-2,3,4-tri-O-acetyl-β-D-galactopyranosiduronoyl)-DL-2-phenylglycin-2-(methoxycarbonyl)cinnamylester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / pyridine / CH₂Cl₂ / 2 h / 25 °C

2: 96 percent / triethylamine / CH₂Cl₂ / 25 °C

With pyridine; triethylamine; In dichloromethane;