Pt((C₆H₅)2PC₆H₄NC(O)C₆H₅)2

Base Information

Chemical Name:Pt((C₆H₅)2PC₆H₄NC(O)C₆H₅)2
CAS No.:91410-08-1
Molecular Formula:C₅₀H₃₈N₂O₂P₂Pt
Molecular Weight:955.891
Hs Code.:

Pt((C<sub>6</sub>H<sub>5</sub>)2PC<sub>6</sub>H<sub>4</sub>NC(O)C<sub>6</sub>H<sub>5</sub>)2

Synonyms:Pt((C₆H₅)2PC₆H₄NC(O)C₆H₅)2

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Chemical Property of Pt((C₆H₅)2PC₆H₄NC(O)C₆H₅)2

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Technology Process of Pt((C₆H₅)2PC₆H₄NC(O)C₆H₅)2

There total 2 articles about Pt((C₆H₅)2PC₆H₄NC(O)C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 91464-49-2,91410-06-9
PtCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

: 91410-08-1
Pt((C₆H₅)2PC₆H₄NC(O)C₆H₅)2

Guidance literature:: With sodium t-butanolate; In acetonitrile; suspending Pt complex and excess of sodium tert-butoxide in dry CH3CN under N2 atmosphere; storage for 48 h;; filtration; evapn. to dryness; recrystn. from CH2Cl2/(C2H5)2O;;

Reference yield:

: 33677-56-4
Pt(dba)2

: 91409-99-3
o-(diphenylphosphino)-N-benzoylaniline

: 91410-08-1
bis(o-(diphenylphosphino)-N-benzoylanilino)platinum(II)

: 102133-35-7
Pt((C₆H₅CHCH)2CO)((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

Guidance literature:: In toluene; N2-atmosphere; addn. of dry toluene to a mixt. of the complex and the aniline; stirring for 1 h;; pptn. on addn. of hexane; filtration; recrystn. (CH2Cl2/hexane); drying(vac., 24-48 h, room temp.); product mixt. not sepd.;
DOI:10.1021/om00138a004

Reference yield: 80.0%

: 91410-08-1
Pt((C₆H₅)2PC₆H₄NC(O)C₆H₅)2

: 91464-49-2
cis-dichlorobis(o-(diphenylphosphino)-N-benzoylaniline)platinum(II)*0.25dichloromethane*diethyl ether

Guidance literature:: With hydrogenchloride; diethyl ether; dichloromethane; In dichloromethane; dissolving Pt complex in CH2Cl2 under N2 atmosphere; bubbling HCl through soln. for 5 min;; removal of HCl excess by purging soln. with vigorous stream of N2; dropwise addn. of (C2H5)2O; pptn.; filtration; washing with (C2H5)2O; dryingin vac.; recrystn. from CH2Cl2/(C2H5)2O; elem. anal.;;