cis-dichlorobis(o-(diphenylphosphino)-N-benzoylaniline)platinum(II)0.25dichloromethanediethyl ether

Base Information

Chemical Name:cis-dichlorobis(o-(diphenylphosphino)-N-benzoylaniline)platinum(II)*0.25dichloromethane*diethyl ether
CAS No.:91464-49-2
Molecular Formula:0CH₂Cl₂*C₄H₁₀O*C₅₀H₄₀Cl₂N₂O₂P₂Pt
Molecular Weight:1124.17
Hs Code.:

Synonyms:cis-dichlorobis(o-(diphenylphosphino)-N-benzoylaniline)platinum(II)*0.25dichloromethane*diethyl ether

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Chemical Property of cis-dichlorobis(o-(diphenylphosphino)-N-benzoylaniline)platinum(II)*0.25dichloromethane*diethyl ether

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Technology Process of cis-dichlorobis(o-(diphenylphosphino)-N-benzoylaniline)platinum(II)*0.25dichloromethane*diethyl ether

There total 5 articles about cis-dichlorobis(o-(diphenylphosphino)-N-benzoylaniline)platinum(II)*0.25dichloromethane*diethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: potassium tetrachloroplatinate

: 91409-99-3
o-(diphenylphosphino)-N-benzoylaniline

: 91464-49-2,91410-06-9
PtCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

Guidance literature:: In water; acetonitrile; dissolving Pt complex in aq. CH3CN under N2 atmosphere; equilibrating on oil bath at 60°C; dropwise addn. of 2 equiv. of ligand in CH3CNover 5 min; stirring for 1 h; pptn.; cooling to room temp.;; filtration; 3 fold washing with water, ethanol and then with pentane; drying in vac.; elem. anal.;;

Reference yield: 80.0%

: 91410-08-1
Pt((C₆H₅)2PC₆H₄NC(O)C₆H₅)2

: 91464-49-2
cis-dichlorobis(o-(diphenylphosphino)-N-benzoylaniline)platinum(II)*0.25dichloromethane*diethyl ether

Guidance literature:: With hydrogenchloride; diethyl ether; dichloromethane; In dichloromethane; dissolving Pt complex in CH2Cl2 under N2 atmosphere; bubbling HCl through soln. for 5 min;; removal of HCl excess by purging soln. with vigorous stream of N2; dropwise addn. of (C2H5)2O; pptn.; filtration; washing with (C2H5)2O; dryingin vac.; recrystn. from CH2Cl2/(C2H5)2O; elem. anal.;;

Reference yield: 50.0%

: 14873-63-3,15617-19-3,51921-56-3
bis(benzonitrile)dichloroplatinum(II)

: 91409-99-3
o-(diphenylphosphino)-N-benzoylaniline

: 91464-49-2,91410-06-9
PtCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

Guidance literature:: In acetonitrile; dissolving Pt complex in CH3CN under N2 atmosphere; equilibrating on oil bath at 60°C; dropwise addn. of 1 equiv. of ligand in CH3CN over 5 min; stirring for 1 h; pptn.; cooling to room temp.;; filtration; 3 fold washing with water, ethanol and then with pentane; drying in vac.;;