phenyl trifluorovinyl sulfone

Base Information

Chemical Name:phenyl trifluorovinyl sulfone
CAS No.:23451-81-2
Molecular Formula:C₈H₅F₃O₂S
Molecular Weight:222.188
Hs Code.:

Synonyms:phenyl trifluorovinyl sulfone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl trifluorovinyl sulfone

Chemical Property:

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Technology Process of phenyl trifluorovinyl sulfone

There total 4 articles about phenyl trifluorovinyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 23451-78-7
1,2,2-trifluorovinyl phenyl sulfide

: 23451-81-2
phenyl trifluorovinyl sulfone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.tet.2004.03.020

Reference yield:

: 3541-14-8
phenyl toluene-4-thiosulfonate

: 23451-81-2
phenyl trifluorovinyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / diethyl ether; hexane / 4 h / -78 °C

1.2: 63 percent / diethyl ether; hexane / 2 h / -45 °C

2.1: 80 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 12 h / 20 °C

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; hexane; dichloromethane;
DOI:10.1016/j.tet.2004.03.020

Reference yield:

: 23451-79-8
[(1,2-dichloro-1,2,2-trifluoroethyl)thio]benzene

: 23451-81-2
phenyl trifluorovinyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: CrO₃, AcOH

2: Zn / dioxane

With chromium(VI) oxide; acetic acid; zinc; In 1,4-dioxane;