(R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid

Base Information

Chemical Name:(R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid
CAS No.:1027932-78-0
Molecular Formula:C₂₃H₂₉NO₅S
Molecular Weight:431.553
Hs Code.:

Synonyms:(R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid

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Chemical Property of (R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid

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Technology Process of (R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid

There total 6 articles about (R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58717-02-5
3-cyclohexyl-D-alanine

: 1027932-78-0
(R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / dioxane; H₂O / Ambient temperature

2: toluene / 3 h / 95 °C

3: K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

4: HCl gas / CH₂Cl₂ / 4 h / Ambient temperature

With hydrogenchloride; potassium carbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm960871c

Reference yield:

: 1026259-81-3
(R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid tert-butyl ester

: 1027932-78-0
(R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid

Guidance literature:: With hydrogenchloride; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jm960871c

Reference yield:

: 100-39-0
benzyl bromide

: 1027932-78-0
(R)-2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-cyclohexyl-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

2: HCl gas / CH₂Cl₂ / 4 h / Ambient temperature

With hydrogenchloride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm960871c