2,7-bis-[3-(benzylamino)propyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Base Information

• Chemical Name: 2,7-bis-[3-(benzylamino)propyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone
• CAS No.: 3436-51-9
• Molecular Formula: C₃₄H₃₂N₄O₄
• Molecular Weight: 560.652

Synonyms:2,7-bis-[3-(benzylamino)propyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Chemical Property of 2,7-bis-[3-(benzylamino)propyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Chemical Property:

Purity/Quality:

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Technology Process of 2,7-bis-[3-(benzylamino)propyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

There total 3 articles about 2,7-bis-[3-(benzylamino)propyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

1,4,5,8-naphthalenetetracarboxylic dianhydride (81-30-1) + N-benzyl-1,3-diaminopropane (13910-48-0) → 2,7-bis-[3-(benzylamino)propyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone (3436-51-9)

Guidance literature:

In isopropyl alcohol; for 2h; Reflux;

DOI:10.1016/j.ejmech.2012.06.045

Reference yield:

benzaldehyde (100-52-7) → 2,7-bis-[3-(benzylamino)propyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone (3436-51-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: toluene / 5 h / Reflux; Dean-Stark

1.2: 4 h / 0 - 20 °C

2.1: isopropyl alcohol / 2 h / Reflux

In isopropyl alcohol; toluene;

DOI:10.1016/j.ejmech.2012.06.045

Reference yield:

→ 2,7-bis-[3-(benzylamino)propyl]benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone (3436-51-9)

Guidance literature:

Dianhydrid (I), Ph-CH2-NH-(CH2)3-NH2 (2 Mol);

upstream raw materials:

benzaldehyde

1,4,5,8-naphthalenetetracarboxylic dianhydride

N-benzyl-1,3-diaminopropane

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