[4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)phenyl]diethoxyphosphine

Base Information

Chemical Name:[4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)phenyl]diethoxyphosphine
CAS No.:1409943-08-3
Molecular Formula:C₁₇H₂₉N₂O₄P
Molecular Weight:356.402
Hs Code.:

Synonyms:[4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)phenyl]diethoxyphosphine

Suppliers and Price of [4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)phenyl]diethoxyphosphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)phenyl]diethoxyphosphine

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Technology Process of [4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)phenyl]diethoxyphosphine

There total 2 articles about [4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)phenyl]diethoxyphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4762-34-9
diethyl (4-bromophenyl)phosphonite

: 1409943-08-3
[4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)phenyl]diethoxyphosphine

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -70 °C / Inert atmosphere

1.2: 7 h / 20 °C / Inert atmosphere

2.1: methanol / 12 h / Reflux; Inert atmosphere

With n-butyllithium; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/ic301394x

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 1409943-08-3
[4-(1,3-dihydroxy-4,4,5,5-tetramethylimidazolidin-2-yl)phenyl]diethoxyphosphine

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -70 °C / Inert atmosphere

1.2: 8 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -70 °C / Inert atmosphere

2.2: 7 h / 20 °C / Inert atmosphere

3.1: methanol / 12 h / Reflux; Inert atmosphere

With n-butyllithium; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/ic301394x