κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride

Base Information

• Chemical Name: κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride
• CAS No.: 1134630-69-5
• Molecular Formula: C₂₄H₃₀N₂*ClH
• Molecular Weight: 382.977
• Mol file: 1134630-69-5.mol

Synonyms:κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride

Chemical Property of κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride

There total 2 articles about κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

2,4-dimethyl-3-ethyl-pyrrole (517-22-6) + phenylacetyl chloride (103-80-0) → κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride (1134630-69-5)

Guidance literature:

In dichloromethane; for 1h; Reflux;

DOI:10.1021/jo900064y

Reference yield:

1,1'-di-κ-(3-ethyl-2,4-dimethyl)pyrrolylstyrene (1134630-71-9) → κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride (1134630-69-5)

Guidance literature:

With hydrogenchloride; In dichloromethane; water;

DOI:10.1021/jo900064y

Reference yield: 85.0%

κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride (1134630-69-5) → C24H29BF2N2 (1219485-13-8)

Guidance literature:

κ2-(4,4'-diethyl-3,3',5,5'-tetramethyl-meso-benzyldipyrrin) hydrochloride; With triethylamine; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane; for 2.08333h; Inert atmosphere;

DOI:10.1021/ol902908j

upstream raw materials:

2,4-dimethyl-3-ethyl-pyrrole

phenylacetyl chloride

1,1'-di-κ-(3-ethyl-2,4-dimethyl)pyrrolylstyrene

Downstream raw materials:

C₂₄H₂₉BF₂N₂