1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide

Base Information

• Chemical Name: 1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide
• CAS No.: 43017-33-0
• Molecular Formula: C₁₅H₁₆P*I
• Molecular Weight: 354.17

Synonyms:1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide

Chemical Property of 1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide

There total 8 articles about 1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dichlorophenylphosphine (644-97-3) → 1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide (43017-33-0)

Guidance literature:

Multi-step reaction with 7 steps

1: (i) Li, Et₂O, (ii) /BRN= 508189/, (iii) H₂O

2: Heating

3: H₂O₂ / CHCl₃; H₂O

4: benzene / Irradiation

5: benzene; acetone / Irradiation

6: AgBF₄ / CHCl₃

7: (i) Si₂Cl₆, benzene, (ii) NaOH, H₂O, (iii) /BRN= 969135/

With silver tetrafluoroborate; dihydrogen peroxide; In chloroform; water; acetone; benzene;

DOI:10.1021/ja00794a027

Reference yield:

1,3,5,7-cyclooctatetraene (629-20-9) → 1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide (43017-33-0)

Guidance literature:

Multi-step reaction with 6 steps

1: (i) Li, Et₂O, (ii) /BRN= 508189/, (iii) H₂O

2: Heating

3: H₂O₂ / CHCl₃; H₂O

4: benzene; acetone / Irradiation

5: AgBF₄ / CHCl₃

6: (i) Si₂Cl₆, benzene, (ii) NaOH, H₂O, (iii) /BRN= 969135/

With silver tetrafluoroborate; dihydrogen peroxide; In chloroform; water; acetone; benzene;

DOI:10.1021/ja00794a027

Reference yield:

anti-9-phenyl-9-phosphabicyclo<4.2.1>nona-2,4,7-trien (13887-07-5) → 1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide (43017-33-0)

Guidance literature:

Multi-step reaction with 5 steps

1: H₂O₂ / CHCl₃; H₂O

2: benzene / Irradiation

3: benzene; acetone / Irradiation

4: AgBF₄ / CHCl₃

5: (i) Si₂Cl₆, benzene, (ii) NaOH, H₂O, (iii) /BRN= 969135/

With silver tetrafluoroborate; dihydrogen peroxide; In chloroform; water; acetone; benzene;

DOI:10.1021/ja00794a027

upstream raw materials:

1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide

methyl iodide

1,3,5,7-cyclooctatetraene

anti-9-phenyl-9-phosphatricyclo<4.2.1.0^2,5>nona-3,7-diene-9-oxide

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