ethyl 2-ethoxy-3-[4-(2-{7-[(hydroxyimino)(phenyl)methyl]-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-4-yl}ethoxy)phenyl]propanoate

Base Information

Chemical Name:ethyl 2-ethoxy-3-[4-(2-{7-[(hydroxyimino)(phenyl)methyl]-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-4-yl}ethoxy)phenyl]propanoate
CAS No.:901114-01-0
Molecular Formula:C₃₀H₃₂N₂O₆S
Molecular Weight:548.66
Hs Code.:

Synonyms:ethyl 2-ethoxy-3-[4-(2-{7-[(hydroxyimino)(phenyl)methyl]-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-4-yl}ethoxy)phenyl]propanoate

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Chemical Property of ethyl 2-ethoxy-3-[4-(2-{7-[(hydroxyimino)(phenyl)methyl]-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-4-yl}ethoxy)phenyl]propanoate

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Technology Process of ethyl 2-ethoxy-3-[4-(2-{7-[(hydroxyimino)(phenyl)methyl]-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-4-yl}ethoxy)phenyl]propanoate

There total 4 articles about ethyl 2-ethoxy-3-[4-(2-{7-[(hydroxyimino)(phenyl)methyl]-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-4-yl}ethoxy)phenyl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ethyl 3-{4-[2-(7-benzoyl-3-oxo-benzo[1,4]thiazin-4-yl)-ethoxy]-phenyl}-2-ethoxypropionate

: 901114-01-0
ethyl 2-ethoxy-3-[4-(2-{7-[(hydroxyimino)(phenyl)methyl]-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-4-yl}ethoxy)phenyl]propanoate

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; for 4h; Heating / reflux;

Reference yield:

: 901113-90-4
7-benzoyl-4H-benzothiazin-3-one

: 901114-01-0
ethyl 2-ethoxy-3-[4-(2-{7-[(hydroxyimino)(phenyl)methyl]-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-4-yl}ethoxy)phenyl]propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C

1.2: 110 °C

2.1: pyridine; hydroxylamine hydrochloride / ethanol / 4 h / Heating / reflux

With pyridine; hydroxylamine hydrochloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 901114-01-0
ethyl 2-ethoxy-3-[4-(2-{7-[(hydroxyimino)(phenyl)methyl]-3-oxo-2,3-dihydro-4H-1,4-benzothiazin-4-yl}ethoxy)phenyl]propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: PPA / 6 h / 160 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C

2.2: 110 °C

3.1: pyridine; hydroxylamine hydrochloride / ethanol / 4 h / Heating / reflux

With pyridine; PPA; hydroxylamine hydrochloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide;