2,3-Diphenyl-4,5-dihydrofuran

Base Information

• Chemical Name: 2,3-Diphenyl-4,5-dihydrofuran
• CAS No.: 54485-06-2
• Molecular Formula: C₁₆H₁₄O
• Molecular Weight: 222.287
• Mol file: 54485-06-2.mol

Synonyms:2,3-Diphenyl-4,5-dihydrofuran

Chemical Property of 2,3-Diphenyl-4,5-dihydrofuran

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-Diphenyl-4,5-dihydrofuran

There total 10 articles about 2,3-Diphenyl-4,5-dihydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

4-(4-methoxyphenoxy)-1,2-diphenylbutan-1-one → 2,3-Diphenyl-4,5-dihydrofuran (54485-06-2)

Guidance literature:

With pyridine; ammonium cerium (IV) nitrate; In water; acetonitrile; at 0 ℃; for 1.5h; Reagent/catalyst; Solvent; Time;

DOI:10.1002/adsc.202101354

Reference yield: 38.0%

diphenyliodonium hexafluorophosphate (58109-40-3) + 4-phenyl-3-butyn-1-ol methyl ether (118554-59-9) → 2,3-Diphenyl-4,5-dihydrofuran (54485-06-2)

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at 60 ℃; Sealed tube; Inert atmosphere;

DOI:10.1039/c4cc08363f

Reference yield: 37.0%

N,N,N-Trimethyl-4-oxo-3,4-diphenyl-butyl-ammoniumiodid → 2,3-Diphenyl-4,5-dihydrofuran (54485-06-2)

Guidance literature:

at 220 - 230 ℃; for 0.5h; under 20 Torr;

DOI:10.1002/ardp.19863190604

upstream raw materials:

4-Dimethylamino-1,2-diphenyl-1-butanon

diphenyliodonium hexafluorophosphate

4-phenyl-3-butyn-1-ol methyl ether

4-phenyl-but-3-yn-1-ol