{(R)-1-[2-((R)-2-tert-Butoxycarbonylamino-3-hydroxy-3,3-diphenyl-propylsulfanyl)-ethylsulfanylmethyl]-2-hydroxy-2,2-diphenyl-ethyl}-carbamic acid tert-butyl ester

Base Information

• Chemical Name: {(R)-1-[2-((R)-2-tert-Butoxycarbonylamino-3-hydroxy-3,3-diphenyl-propylsulfanyl)-ethylsulfanylmethyl]-2-hydroxy-2,2-diphenyl-ethyl}-carbamic acid tert-butyl ester
• CAS No.: 209342-91-6
• Molecular Formula: C₄₂H₅₂N₂O₆S₂
• Molecular Weight: 745.017

Synonyms:{(R)-1-[2-((R)-2-tert-Butoxycarbonylamino-3-hydroxy-3,3-diphenyl-propylsulfanyl)-ethylsulfanylmethyl]-2-hydroxy-2,2-diphenyl-ethyl}-carbamic acid tert-butyl ester

Chemical Property of {(R)-1-[2-((R)-2-tert-Butoxycarbonylamino-3-hydroxy-3,3-diphenyl-propylsulfanyl)-ethylsulfanylmethyl]-2-hydroxy-2,2-diphenyl-ethyl}-carbamic acid tert-butyl ester

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Technology Process of {(R)-1-[2-((R)-2-tert-Butoxycarbonylamino-3-hydroxy-3,3-diphenyl-propylsulfanyl)-ethylsulfanylmethyl]-2-hydroxy-2,2-diphenyl-ethyl}-carbamic acid tert-butyl ester

There total 1 articles about {(R)-1-[2-((R)-2-tert-Butoxycarbonylamino-3-hydroxy-3,3-diphenyl-propylsulfanyl)-ethylsulfanylmethyl]-2-hydroxy-2,2-diphenyl-ethyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

phenylmagnesium bromide (100-58-3) + (R)-2-tert-Butoxycarbonylamino-3-[2-((R)-2-tert-butoxycarbonylamino-2-methoxycarbonyl-ethylsulfanyl)-ethylsulfanyl]-propionic acid methyl ester (209342-88-1) → {(R)-1-[2-((R)-2-tert-Butoxycarbonylamino-3-hydroxy-3,3-diphenyl-propylsulfanyl)-ethylsulfanylmethyl]-2-hydroxy-2,2-diphenyl-ethyl}-carbamic acid tert-butyl ester (209342-91-6)

Guidance literature:

In tetrahydrofuran; for 12h; Heating;

DOI:10.1016/S0957-4166(98)00106-2

Reference yield: 77.0%

{(R)-1-[2-((R)-2-tert-Butoxycarbonylamino-3-hydroxy-3,3-diphenyl-propylsulfanyl)-ethylsulfanylmethyl]-2-hydroxy-2,2-diphenyl-ethyl}-carbamic acid tert-butyl ester (209342-91-6) → (2R,9R)-2,9-di-(monomethyl)-amino-1,1,10,10-tetraphenyl-4,7-dithia-decan-1,10-diol

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 24h; Heating;

DOI:10.1016/S0957-4166(98)00106-2

Reference yield: 74.0%

{(R)-1-[2-((R)-2-tert-Butoxycarbonylamino-3-hydroxy-3,3-diphenyl-propylsulfanyl)-ethylsulfanylmethyl]-2-hydroxy-2,2-diphenyl-ethyl}-carbamic acid tert-butyl ester (209342-91-6) → (2R,9R)-2,9-diamino-1,1,10,10-tetraphenyl-4,7-dithia-decan-1,10-diol

Guidance literature:

With trifluoroacetic acid; In dichloromethane; Ambient temperature;

DOI:10.1016/S0957-4166(98)00106-2

upstream raw materials:

phenylmagnesium bromide

(R)-2-tert-Butoxycarbonylamino-3-[2-((R)-2-tert-butoxycarbonylamino-2-methoxycarbonyl-ethylsulfanyl)-ethylsulfanyl]-propionic acid methyl ester

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