4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid

Base Information

Chemical Name:4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid
CAS No.:329785-21-9
Molecular Formula:C₁₆H₁₁Cl₄NO₅
Molecular Weight:439.079
Hs Code.:

Synonyms:4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid

Suppliers and Price of 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid

There total 4 articles about 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 329785-20-8
methyl 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetate

: 329785-21-9
4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid

Guidance literature:: With lithium hydroxide; In ethanol; at 20 ℃; for 24h;
DOI:10.1021/jf0010578

Reference yield:

: 87-87-6
2,3,5,6-tetrachlorobenzene-1,4-diol

: 329785-21-9
4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / aq. NaOH / 4 h / 80 °C

2: 59 percent / EDC; Et₃N / dimethylformamide / 22 h / 20 °C

3: 62 percent / LiOH / ethanol / 24 h / 20 °C

With lithium hydroxide; sodium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jf0010578

Reference yield:

: 951-11-1
(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetic acid

: 329785-21-9
4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / EDC; Et₃N / dimethylformamide / 22 h / 20 °C

2: 62 percent / LiOH / ethanol / 24 h / 20 °C

With lithium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jf0010578