methyl 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetate

Base Information

Chemical Name:methyl 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetate
CAS No.:329785-20-8
Molecular Formula:C₁₇H₁₃Cl₄NO₅
Molecular Weight:453.106
Hs Code.:

Synonyms:methyl 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetate

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Chemical Property of methyl 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetate

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Technology Process of methyl 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetate

There total 2 articles about methyl 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 951-11-1
(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetic acid

: 83528-16-9
methyl 2-(4-aminophenyl)acetate hydrochloride

: 329785-20-8
methyl 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetate

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 22h;
DOI:10.1021/jf0010578

Reference yield:

: 87-87-6
2,3,5,6-tetrachlorobenzene-1,4-diol

: 329785-20-8
methyl 4-[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]aminophenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / aq. NaOH / 4 h / 80 °C

2: 59 percent / EDC; Et₃N / dimethylformamide / 22 h / 20 °C

With sodium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jf0010578