(E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(4-methyl-N-tosylbenzenesulfonamide)

Base Information

• Chemical Name: (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(4-methyl-N-tosylbenzenesulfonamide)
• CAS No.: 1379605-97-6
• Molecular Formula: C₃₈H₃₈N₂O₈S₄
• Molecular Weight: 778.992
• Mol file: 1379605-97-6.mol

Synonyms:(E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(4-methyl-N-tosylbenzenesulfonamide)

Chemical Property of (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(4-methyl-N-tosylbenzenesulfonamide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(4-methyl-N-tosylbenzenesulfonamide)

There total 7 articles about (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(4-methyl-N-tosylbenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(E)-buta-1,3-dienylbenzene (16939-57-4) + acetoxy((4-methyl)-N-tosylbenzenesulfonamidyl)iodosobenzene (1345824-06-7) + di(4-tosyl)amine (3695-00-9) → (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(4-methyl-N-tosylbenzenesulfonamide) (1379605-97-6)

Guidance literature:

((4-methyl-N-tosylphenyl)sulfonamido)(phenyl)-λ³-iodanyl acetate; di(4-tosyl)amine; In dichloromethane; at 20 ℃; for 0.0833333h;

(E)-buta-1,3-dienylbenzene; In dichloromethane; at 20 ℃; for 12h; regioselective reaction;

DOI:10.1002/chem.201103435

Reference yield: 75.0%

→ (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(4-methyl-N-tosylbenzenesulfonamide) (1379605-97-6)

Guidance literature:

Reference yield: 73.0%

(E)-buta-1,3-dienylbenzene (16939-57-4) + di(4-tosyl)amine (3695-00-9) → (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(4-methyl-N-tosylbenzenesulfonamide) (1379605-97-6)

Guidance literature:

di(4-tosyl)amine; With [bis(acetoxy)iodo]benzene; In dichloromethane; at 20 ℃; for 0.0833333h;

(E)-buta-1,3-dienylbenzene; In dichloromethane; at 20 ℃; for 12h; regioselective reaction;

DOI:10.1002/chem.201103435

upstream raw materials:

(E)-3-phenylpropenal

(E)-buta-1,3-dienylbenzene

acetoxy((4-methyl)-N-tosylbenzenesulfonamidyl)iodosobenzene

di(4-tosyl)amine