2-<1'-methyl-2'-(2'',6'',6''-trimethyl-2''-cyclohexenyl)vinyl>-1,3-dithiane

Base Information

Chemical Name:2-<1'-methyl-2'-(2'',6'',6''-trimethyl-2''-cyclohexenyl)vinyl>-1,3-dithiane
CAS No.:109629-43-8
Molecular Formula:C₁₆H₂₆S₂
Molecular Weight:282.514
Hs Code.:

Synonyms:2-<1'-methyl-2'-(2'',6'',6''-trimethyl-2''-cyclohexenyl)vinyl>-1,3-dithiane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<1'-methyl-2'-(2'',6'',6''-trimethyl-2''-cyclohexenyl)vinyl>-1,3-dithiane

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Technology Process of 2-<1'-methyl-2'-(2'',6'',6''-trimethyl-2''-cyclohexenyl)vinyl>-1,3-dithiane

There total 4 articles about 2-<1'-methyl-2'-(2'',6'',6''-trimethyl-2''-cyclohexenyl)vinyl>-1,3-dithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 109-80-8
1.3-propanedithiol

: 109629-42-7,67801-14-3
(E)-2-Methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propenal

: 109629-43-8
2-<1'-methyl-2'-(2'',6'',6''-trimethyl-2''-cyclohexenyl)vinyl>-1,3-dithiane

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; acetic acid; 1.) 45 min, 0 deg C, 2.) 3 h, room temperature;
DOI:10.1002/hlca.19860690612

Reference yield:

: 15789-90-9
alpha-isomethylionone

: 109629-43-8
2-<1'-methyl-2'-(2'',6'',6''-trimethyl-2''-cyclohexenyl)vinyl>-1,3-dithiane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) I₂, 2.) 2N NaOH / 1.) pyridine, 100 deg C, 1 h, 2.) 100 deg C

2: 65 percent / LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

3: 87 percent / MnO₂ / hexane

4: 75 percent / BF₃*Et₂O / acetic acid; CH₂Cl₂ / 1.) 45 min, 0 deg C, 2.) 3 h, room temperature

With manganese(IV) oxide; sodium hydroxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; iodine; In diethyl ether; hexane; dichloromethane; acetic acid;
DOI:10.1002/hlca.19860690612

Reference yield:

: 109629-41-6
(E)-2-Methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-prop-2-en-1-ol

: 109629-43-8
2-<1'-methyl-2'-(2'',6'',6''-trimethyl-2''-cyclohexenyl)vinyl>-1,3-dithiane

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / MnO₂ / hexane

2: 75 percent / BF₃*Et₂O / acetic acid; CH₂Cl₂ / 1.) 45 min, 0 deg C, 2.) 3 h, room temperature

With manganese(IV) oxide; boron trifluoride diethyl etherate; In hexane; dichloromethane; acetic acid;
DOI:10.1002/hlca.19860690612