2-(2-Chlorophenyl)-N-(3-chlorophenyl)-2-formylaminoacetamide

Base Information

Chemical Name:2-(2-Chlorophenyl)-N-(3-chlorophenyl)-2-formylaminoacetamide
CAS No.:5770-91-2
Molecular Formula:C₁₄H₁₂S₄Sn
Molecular Weight:427.223
Hs Code.:
DSSTox Substance ID:DTXSID10973296

Synonyms:5770-91-2;TimTec1_002763;Oprea1_608093;DTXSID10973296;HMS1541N13;AKOS005458276;NCGC00173772-01;SR-01000519459;SR-01000519459-1;2-(2-CHLOROPHENYL)-N-(3-CHLOROPHENYL)-2-FORMYLAMINOACETAMIDE;2-(2-Chlorophenyl)-N-(3-chlorophenyl)-2-[(hydroxymethylidene)amino]ethanimidic acid

Suppliers and Price of 2-(2-Chlorophenyl)-N-(3-chlorophenyl)-2-formylaminoacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-Chlorophenyl)-N-(3-chlorophenyl)-2-formylaminoacetamide

Chemical Property:

Vapor Pressure:1.52E-14mmHg at 25°C
Boiling Point:539.9°Cat760mmHg
Flash Point:280.3°C
Density:1.405g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:322.0275830
Heavy Atom Count:21
Complexity:368

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(C(=O)NC2=CC(=CC=C2)Cl)NC=O)Cl

Technology Process of 2-(2-Chlorophenyl)-N-(3-chlorophenyl)-2-formylaminoacetamide

There total 2 articles about 2-(2-Chlorophenyl)-N-(3-chlorophenyl)-2-formylaminoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

: 10026-06-9
tin (IV) chloride pentahydrate

: 496-74-2
3,4-dimercaptotoluene

: 13241-47-9,5770-91-2
bis(toluene-3,4-dithiolato)tin(IV)

Guidance literature:: In water; ligand was added to soln. of SnCl4*5H2O in water at room temp., soln. was stirred for 1.5 h; filtered, under suction, washed with H2O, air dried;

Reference yield:

: 496-74-2
3,4-dimercaptotoluene

: 1,3-dithia-2,2-dichlorostannyl-[3]ferrocenophane

: 13241-47-9,5770-91-2
bis(toluene-3,4-dithiolato)tin(IV)

: Fe(C₅H₄S)2SnS₂C₆H₃CH₃

: bis(ferrocene-1,1'-dithiolato)-stannane

Guidance literature:: With BuLi; In tetrahydrofuran; hexane; addn. of 2 equiv. BuLi (in hexane) to dithiol, addn. to ferrocene derivative; recrystn. (CHCl3);
DOI:10.1016/s0020-1693(99)00133-4

Reference yield: 89.7%

: 13241-47-9,5770-91-2
bis(toluene-3,4-dithiolato)tin(IV)

: 1779-49-3
Methyltriphenylphosphonium bromide

: methyltriphenylphosphonium bis(4-methylbenzene-1,2-dithiolato)bromostannate

Guidance literature:: In acetonitrile; suspension of Sn(C7H6S2)2 and H3CPPh3Br in acetonitrile stirred at room temp. for 0.5 h; obtained dark yellow soln. evaporated; crystalline residue washed, filtered, dried and recrystallized from acetonitrile at 0 ° C;
DOI:10.1021/ja00212a027