4-bis-(phenylthio)methyl-4-hydroxy-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole

Base Information

Chemical Name:4-bis-(phenylthio)methyl-4-hydroxy-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole
CAS No.:106507-71-5
Molecular Formula:C₂₈H₂₇NO₃S₃
Molecular Weight:521.725
Hs Code.:

Synonyms:4-bis-(phenylthio)methyl-4-hydroxy-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bis-(phenylthio)methyl-4-hydroxy-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole

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Technology Process of 4-bis-(phenylthio)methyl-4-hydroxy-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole

There total 1 articles about 4-bis-(phenylthio)methyl-4-hydroxy-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35577-89-0
1-[(4-methylbenzene)sulfonyl]-4,5,6,7-tetrahydro-1H-indol-4-one

: 3561-67-9
bis(phenylthio)methane

: 106507-71-5
4-bis-(phenylthio)methyl-4-hydroxy-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 1.5 h, 2.) THF, hexane, from -78 deg C to RT;

Reference yield: 80.8%

: 106507-71-5
4-bis-(phenylthio)methyl-4-hydroxy-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole

: 106507-72-6
5-phenylthio-4-(phenylthio)methylidene-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; Ambient temperature;

Reference yield:

: 106507-71-5
4-bis-(phenylthio)methyl-4-hydroxy-1-(p-toluenesulfonyl)-4,5,6,7-tetrahydroindole

: 79681-04-2
1-[(4-methyl-phenyl)-sulfonyl]-1H-indol-4-carboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 80.8 percent / TsOH*H₂O / CH₂Cl₂ / Ambient temperature

2: 53.8 percent / CuCl₂ / methanol; tetrahydrofuran; H₂O / 50 - 60 °C

With toluene-4-sulfonic acid; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water;