3',4'-di-O-acetyl-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

Base Information

Chemical Name:3',4'-di-O-acetyl-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine
CAS No.:942420-54-4
Molecular Formula:C₃₅H₄₃N₁₁O₁₂
Molecular Weight:809.793
Hs Code.:

Synonyms:3',4'-di-O-acetyl-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

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Chemical Property of 3',4'-di-O-acetyl-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

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Technology Process of 3',4'-di-O-acetyl-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

There total 3 articles about 3',4'-di-O-acetyl-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₄N₁₀O₈

: 942420-52-2
(S)-2-O-benzyl-4-(benzyloxaycarbonylamino)butyric acid

: 942420-54-4
3',4'-di-O-acetyl-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jo062588j

Reference yield:

: 942420-48-6
3',4'-di-O-acetyl-1-N-tert-butoxycarbonyl-3,2',6'-trizidone-5,6-O-cyclohexylideneamine

: 942420-54-4
3',4'-di-O-acetyl-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂; H₂O / 7 h / 20 °C

2: 0.37 g / EDC; HOBt; Et₃N / dimethylformamide / 20 °C

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo062588j

Reference yield:

: 182554-06-9
5,6,3',4'-tetra-O-acetyl-1,3,2',6'-tetrazidoneamine

: 942420-54-4
3',4'-di-O-acetyl-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanoyl]-3,2',6'-triazidoneamine

Guidance literature:: Multi-step reaction with 3 steps

1: TFA / CH₂Cl₂; H₂O / 7 h / 20 °C

2: 0.37 g / EDC; HOBt; Et₃N / dimethylformamide / 20 °C

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo062588j