5,6,3',4'-tetra-O-acetyl-1,3,2',6'-tetrazidoneamine

Base Information

Chemical Name:5,6,3',4'-tetra-O-acetyl-1,3,2',6'-tetrazidoneamine
CAS No.:182554-06-9
Molecular Formula:C₂₀H₂₆N₁₂O₁₀
Molecular Weight:594.501
Hs Code.:

Synonyms:5,6,3',4'-tetra-O-acetyl-1,3,2',6'-tetrazidoneamine

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Chemical Property of 5,6,3',4'-tetra-O-acetyl-1,3,2',6'-tetrazidoneamine

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Technology Process of 5,6,3',4'-tetra-O-acetyl-1,3,2',6'-tetrazidoneamine

There total 6 articles about 5,6,3',4'-tetra-O-acetyl-1,3,2',6'-tetrazidoneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-24-7
acetic anhydride

: 106-45-6
para-thiocresol

: 474266-81-4
hexaazido-hepta-O-acetyl neomycin

: 182554-06-9
5,6,3',4'-tetra-O-acetyl-1,3,2',6'-tetrazidoneamine

: 474266-82-5
acetic acid 4-acetoxy-6-(4-acetoxy-2-acetoxymethyl-5-p-tolylsulfanyl-tetrahydrofuran-3-yloxy)-5-azido-2-azidomethyl-tetrahydro-pyran-3-yl ester

Guidance literature:: para-thiocresol; hexaazido-hepta-O-acetyl neomycin; With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 15h;

acetic anhydride; With pyridine; dmap; Further stages.;
DOI:10.1021/ol026548n