allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Base Information

Chemical Name:allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside
CAS No.:106284-64-4
Molecular Formula:C₅₇H₆₀O₁₂
Molecular Weight:937.096
Hs Code.:

Synonyms:allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

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Chemical Property of allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

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Technology Process of allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

There total 5 articles about allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 106238-71-5
allyl O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

: 106284-64-4
allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In chloroform; at -10 ℃; for 0.5h;
DOI:10.1016/0008-6215(86)80014-3

Reference yield: 97.0%

: 106238-72-6
allyl O-<2-O-benzoyl-4,6-di-O-benzyl-3-O-(tetrahydro-2-pyranyl)-β-D-glactopyranosyl>-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

: 106284-64-4
allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Guidance literature:: With water; In methanol; acetic acid; at 100 ℃; for 1h;
DOI:10.1016/0008-6215(86)80014-3

Reference yield:

: 61236-87-1
allyl 2,4,6-tri-O-benzyl-α-D-galactopyranoside

: 106284-64-4
allyl O-(2-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / silver trifluoromethanesulfonate, tetramethylurea / CH₂Cl₂

2: 97.5 percent / borotrifluoride etherate / CHCl₃ / 0.5 h / -10 °C

With boron trifluoride diethyl etherate; silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; chloroform;
DOI:10.1016/0008-6215(86)80014-3