6-Methoxy-3,5-cyclocholestane

Base Information

Chemical Name:6-Methoxy-3,5-cyclocholestane
CAS No.:2867-93-8
Molecular Formula:C28H48O
Molecular Weight:400.689
Hs Code.:
NSC Number:134933
DSSTox Substance ID:DTXSID90951330
Mol file:2867-93-8.mol

Synonyms:6 beta-methoxy-3 alpha,5 alpha-cyclocholestane;6 beta-methoxy-i-cholesterol

Suppliers and Price of 6-Methoxy-3,5-cyclocholestane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
EPI-CHOLESTERYL METHYL ETHER Aldrich
1g
$ 144.00

Sigma-Aldrich
i-Cholesteryl methyl ether ~95%
1g
$ 139.00

American Custom Chemicals Corporation
I-CHOLESTERYL METHYL ETHER 95.00%
1G
$ 668.23

American Custom Chemicals Corporation
I-CHOLESTERYL METHYL ETHER 95.00%
250MG
$ 568.53

Total 10 raw suppliers

Chemical Property of 6-Methoxy-3,5-cyclocholestane

Chemical Property:

Vapor Pressure:2.11E-07mmHg at 25°C
Refractive Index:1.519
Boiling Point:436.2 °C at 760 mmHg
Flash Point:217.3 °C
PSA：9.23000
Density:0.98 g/cm³
LogP:7.73260
Storage Temp.:−20°C
XLogP3:9.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:6
Exact Mass:400.370516150
Heavy Atom Count:29
Complexity:626

Purity/Quality:

99% ^*data from raw suppliers

EPI-CHOLESTERYL METHYL ETHER Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CC(C)CCCC(C)C1CCC2C1(CCC3C2CC(C45C3(CCC4C5)C)OC)C

Technology Process of 6-Methoxy-3,5-cyclocholestane

There total 2 articles about 6-Methoxy-3,5-cyclocholestane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2203-80-7
5-methylhex-1-yne

: 2867-93-8,60175-48-6,84985-77-3,103365-95-3,122406-68-2
(6R,10aR)-6-((R)-1,5-Dimethyl-hexyl)-10-methoxy-3a,5a-dimethyl-hexadecahydro-cyclopenta[a]cyclopropa[2,3]cyclopenta[1,2-f]naphthalene

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) LDA / 1.) THF, 0 deg C

2: 85 percent / pyridine

3: Li₂CO₃ / chlorobenzene / Heating

4: 85 percent / tetrahydrofuran / 0 °C

5: 90 percent / Li, ethylamine / -75 °C

6: H₂ / PtO₂ / ethyl acetate; acetic acid

With hydrogen; lithium; lithium carbonate; ethylamine; lithium diisopropyl amide; platinum(IV) oxide; In tetrahydrofuran; pyridine; acetic acid; ethyl acetate; chlorobenzene;
DOI:10.1016/S0040-4039(00)85693-2

Reference yield:

: 2203-80-7
5-methylhex-1-yne

: 2867-93-8,60175-48-6,84985-77-3,103365-95-3,122406-68-2
(6R,10aR)-6-((S)-1,5-Dimethyl-hexyl)-10-methoxy-3a,5a-dimethyl-hexadecahydro-cyclopenta[a]cyclopropa[2,3]cyclopenta[1,2-f]naphthalene

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) LDA / 1.) THF, 0 deg C

2: 85 percent / pyridine

3: Li₂CO₃ / chlorobenzene / Heating

4: 85 percent / tetrahydrofuran / 0 °C

5: 90 percent / Li, ethylamine / -75 °C

6: H₂ / PtO₂ / ethyl acetate; acetic acid

With hydrogen; lithium; lithium carbonate; ethylamine; lithium diisopropyl amide; platinum(IV) oxide; In tetrahydrofuran; pyridine; acetic acid; ethyl acetate; chlorobenzene;
DOI:10.1016/S0040-4039(00)85693-2