N₂-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N₂-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N₁-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

Base Information

• Chemical Name: N₂-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N₂-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N₁-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide
• CAS No.: 1190896-17-3
• Molecular Formula: C₃₂H₄₂FN₇O₅
• Molecular Weight: 623.728

Synonyms:N₂-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N₂-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N₁-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

Chemical Property of N₂-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N₂-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N₁-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

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Technology Process of N₂-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N₂-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N₁-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide

There total 1 articles about N₂-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N₂-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N₁-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]iminodiacetic acid (1190891-17-8) + 5-fluoro-N-methyl-1,3-dihydro-2H-isoindol-2-amine hydrochloride (1190890-20-0) + (2-aminoethyl)(ethyl)carbamic acid tert-butyl ester (105628-63-5) → N2-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N2-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide (1190896-17-3)

Guidance literature:

With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield: 86.0%

N2-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N2-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N1-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide (1190896-17-3) → N2-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N2-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N1-[2-(ethylamino)ethyl]glycinamide dihydrochloride

Guidance literature:

N₂-{2-[(5-fluoro-1,3-dihydro-2H-isoindol-2-yl)(methyl)amino]-2-oxoethyl}-N₂-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]-N₁-{2-[(tert-butoxycarbonyl)(ethyl)amino]ethyl}glycinamide; With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 0 - 30 ℃; for 2h;

With sodium hydroxide; In 1,4-dioxane; dichloromethane; chloroform; water;

With hydrogenchloride; In diethyl ether; ethyl acetate;

upstream raw materials:

N-[2-methyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenyl]iminodiacetic acid

5-fluoro-N-methyl-1,3-dihydro-2H-isoindol-2-amine hydrochloride

(2-aminoethyl)(ethyl)carbamic acid tert-butyl ester

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