N⁶-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine

Base Information

Chemical Name:N⁶-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine
CAS No.:163631-85-4
Molecular Formula:C₄₉H₄₀N₆O₆
Molecular Weight:808.893
Hs Code.:

N<sup>6</sup>-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine

Synonyms:N⁶-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine

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Chemical Property of N⁶-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine

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Technology Process of N⁶-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine

There total 3 articles about N⁶-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 163631-82-1
6-fluoro-1-nitropyrene

: 3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine

: 163631-85-4
N⁶-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 140 ℃; for 24h;
DOI:10.1021/tx00047a009

Reference yield:

: 1606-67-3
1-aminopyrene

: 163631-85-4
N⁶-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine

Guidance literature:: Multi-step reaction with 3 steps

1.1: HBF₄; NaNO₂ / acetonitrile; H₂O

1.2: 18 percent / 160 °C

2.1: HNO₃ / acetic acid / 0.5 h / 20 °C

3.1: 31 percent / K₂CO₃ / dimethylsulfoxide / 24 h / 140 °C

With tetrafluoroboric acid; nitric acid; potassium carbonate; sodium nitrite; In water; acetic acid; dimethyl sulfoxide; acetonitrile; 1.1: Diazotization / 1.2: Decomposition / 2.1: Nitration / 3.1: Addition;
DOI:10.1021/tx00047a009

Reference yield:

: 1691-65-2
1-fluoropyrene

: 163631-85-4
N⁶-(1-nitropyren-6-yl)-3'-O-(tetrahydrofuranyl)-5'-O-trityldeoxyadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: HNO₃ / acetic acid / 0.5 h / 20 °C

2: 31 percent / K₂CO₃ / dimethylsulfoxide / 24 h / 140 °C

With nitric acid; potassium carbonate; In acetic acid; dimethyl sulfoxide; 1: Nitration / 2: Addition;
DOI:10.1021/tx00047a009