C₂₉H₃₇N₅O₆

Base Information

Chemical Name:C₂₉H₃₇N₅O₆
CAS No.:1295471-27-0
Molecular Formula:C₂₉H₃₇N₅O₆
Molecular Weight:551.643
Hs Code.:

C<sub>29</sub>H<sub>37</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:C₂₉H₃₇N₅O₆

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Chemical Property of C₂₉H₃₇N₅O₆

Chemical Property:

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Technology Process of C₂₉H₃₇N₅O₆

There total 7 articles about C₂₉H₃₇N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1295471-61-2
C₂₆H₃₃N₅O₆

: 77-76-9
2,2-dimethoxy-propane

: 1295471-27-0
C₂₉H₃₇N₅O₆

Guidance literature:: With CSA; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-56-5
C₁₇H₂₀N₄O₅

: 1295471-27-0
C₂₉H₃₇N₅O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: zinc trifluoromethanesulfonate; acetic acid / 48 h / 80 °C

1.2: 1 h / 0 - 20 °C

2.1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C

3.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

4.1: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C

5.1: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C

6.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

7.1: CSA / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; dmap; trifluoromethylsulfonic anhydride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; zinc trifluoromethanesulfonate; acetic acid; triethylamine; ytterbium(III) triflate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-59-8
C₁₇H₂₂N₄O₆

: 1295471-27-0
C₂₉H₃₇N₅O₆

Guidance literature:: Multi-step reaction with 6 steps

1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C

2: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

3: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C

4: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C

5: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

6: CSA / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; dmap; trifluoromethylsulfonic anhydride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; triethylamine; ytterbium(III) triflate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201008079