thiophosphoric acid O,O'-diethyl ester S-(2-nitrophenyl) ester

Base Information Edit

Chemical Name:thiophosphoric acid O,O'-diethyl ester S-(2-nitrophenyl) ester
CAS No.:4184-46-7
Molecular Formula:C₁₀H₁₄NO₅PS
Molecular Weight:291.265
Hs Code.:
Mol file:4184-46-7.mol

Synonyms:thiophosphoric acid O,O'-diethyl ester S-(2-nitrophenyl) ester

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Chemical Property of thiophosphoric acid O,O'-diethyl ester S-(2-nitrophenyl) ester Edit

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Technology Process of thiophosphoric acid O,O'-diethyl ester S-(2-nitrophenyl) ester

There total 3 articles about thiophosphoric acid O,O'-diethyl ester S-(2-nitrophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 88-74-4
2-nitro-aniline

: 762-04-9
phosphonic acid diethyl ester

: 4184-46-7
thiophosphoric acid O,O'-diethyl ester S-(2-nitrophenyl) ester

Guidance literature:: phosphonic acid diethyl ester; With sulfur; triethylamine; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

2-nitro-aniline; With tert.-butylnitrite; methanesulfonic acid; In dimethyl sulfoxide; at 20 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c7cy00467b