Benzaldehyde 2-bromophenylhydrazone

Base Information

• Chemical Name: Benzaldehyde 2-bromophenylhydrazone
• CAS No.: 10407-12-2
• Molecular Formula: C13H11 Br N2
• Molecular Weight: 275.1438
• Mol file: 10407-12-2.mol

Synonyms:BRN 1819294;Benzaldehyde 2-bromophenylhydrazone;Benzaldehyde, (o-bromophenyl)hydrazone;10407-12-2;LS-24936

Chemical Property of Benzaldehyde 2-bromophenylhydrazone

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 369.2°Cat760mmHg
• PKA: 13.00±0.10(Predicted)
• Flash Point: 177.1°C
• PSA: 24.39000
• Density: 1.33g/cm³
• LogP: 3.96810
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 274.01056
• Heavy Atom Count: 16
• Complexity: 224

Purity/Quality:

BENZALDEHYDE(ORTHO-BROMOPHENYL)HYDRAZONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C=NNC2=CC=CC=C2Br
• Isomeric SMILES: C1=CC=C(C=C1)/C=N/NC2=CC=CC=C2Br

Technology Process of Benzaldehyde 2-bromophenylhydrazone

There total 1 articles about Benzaldehyde 2-bromophenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-benzylidene-2-(2-bromophenyl)hydrazine (10407-12-2)

Guidance literature:

Benzaldehyd, 2-Brom-phenylhydrazin-hydrochlorid;

DOI:10.1021/jo01281a057

Reference yield: 61.0%

1-benzylidene-2-(2-bromophenyl)hydrazine (10407-12-2) + benzylamine (100-46-9) → C20H14BrN3

Guidance literature:

With ferrocene; sodium acetate; tert-butylammonium hexafluorophosphate(V); In 1,2-dichloro-ethane; at 55 ℃; for 11.5h; Electrolysis; Inert atmosphere; Green chemistry;

DOI:10.1002/open.202100268

Reference yield: 45.0%

tetrachloromethane (56-23-5) + 1-benzylidene-2-(2-bromophenyl)hydrazine (10407-12-2) → (E)-1-(2-bromophenyl)-2-(2,2-dichloro-1-phenylvinyl)diazene

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; copper(l) chloride; In dimethyl sulfoxide; at 20 ℃; for 3h; Cooling;

DOI:10.1021/acs.orglett.8b03227

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