4a-Morpholin-4-yl-1,3-diphenyl-6,7,8,8a-tetrahydro-1H,4aH-benzo[1,3,4]oxadiazin-5-one

Base Information

• Chemical Name: 4a-Morpholin-4-yl-1,3-diphenyl-6,7,8,8a-tetrahydro-1H,4aH-benzo[1,3,4]oxadiazin-5-one
• CAS No.: 84999-57-5
• Molecular Formula: C₂₃H₂₅N₃O₃
• Molecular Weight: 391.47

Synonyms:4a-Morpholin-4-yl-1,3-diphenyl-6,7,8,8a-tetrahydro-1H,4aH-benzo[1,3,4]oxadiazin-5-one

Chemical Property of 4a-Morpholin-4-yl-1,3-diphenyl-6,7,8,8a-tetrahydro-1H,4aH-benzo[1,3,4]oxadiazin-5-one

Chemical Property:

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Technology Process of 4a-Morpholin-4-yl-1,3-diphenyl-6,7,8,8a-tetrahydro-1H,4aH-benzo[1,3,4]oxadiazin-5-one

There total 2 articles about 4a-Morpholin-4-yl-1,3-diphenyl-6,7,8,8a-tetrahydro-1H,4aH-benzo[1,3,4]oxadiazin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(E)-phenyl(phenyldiazenyl)methanone (952-53-4) + 2-morpholinocyclohex-2-enone (23740-64-9) → 4a-Morpholin-4-yl-1,3-diphenyl-6,7,8,8a-tetrahydro-1H,4aH-benzo[1,3,4]oxadiazin-5-one (84999-57-5)

Guidance literature:

In benzene; at 0 ℃;

Reference yield:

2-hydroxy-2-cyclohexen-1-one (10316-66-2) → 4a-Morpholin-4-yl-1,3-diphenyl-6,7,8,8a-tetrahydro-1H,4aH-benzo[1,3,4]oxadiazin-5-one (84999-57-5)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / Heating

2: 80 percent / benzene / 0 °C

In benzene;

Reference yield: 100.0%

4a-Morpholin-4-yl-1,3-diphenyl-6,7,8,8a-tetrahydro-1H,4aH-benzo[1,3,4]oxadiazin-5-one (84999-57-5) → Benzoic acid N'-(2-morpholin-4-yl-3-oxo-cyclohex-1-enyl)-N'-phenyl-hydrazide (84999-63-3)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 4h;

upstream raw materials:

(E)-phenyl(phenyldiazenyl)methanone

2-morpholinocyclohex-2-enone

2-hydroxy-2-cyclohexen-1-one

Downstream raw materials:

Benzoic acid N'-(2-morpholin-4-yl-3-oxo-cyclohex-1-enyl)-N'-phenyl-hydrazide

N-benzoyl-N'-phenylhydrazine

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