6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide

Base Information

• Chemical Name: 6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide
• CAS No.: 1361952-36-4
• Molecular Formula: C₅₈H₇₃N₅O₅Si
• Molecular Weight: 948.334

Synonyms:6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide

Chemical Property of 6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide

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Technology Process of 6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide

There total 1 articles about 6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-bromohexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide + (R)-5-(2-(benzylamino)-1-((tert-butyldimethylsilyl)oxy)ethyl)-8-(benzyloxy)quinolin-2(1H) one (743460-26-6) → 6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide (1361952-36-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 80 ℃; for 24h;

Reference yield:

6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-(tert-butyldimethylsilanyloxy)ethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide (1361952-36-4) → 6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-hydroxyethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide (1361952-37-5)

Guidance literature:

With triethylamine tris(hydrogen fluoride); In dichloromethane; for 10h;

upstream raw materials:

(R)-5-(2-(benzylamino)-1-((tert-butyldimethylsilyl)oxy)ethyl)-8-(benzyloxy)quinolin-2(1H) one

Downstream raw materials:

6-{benzyl-[(R)-2-(8-benzyloxy-2-oxo-1,2-dihydroquinolin-5-yl)-2-hydroxyethyl]amino}hexanoic acid {2-[(S)-3-(carbamoyldiphenylmethyl)pyrrolidin-1-yl]ethyl}methylamide

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