6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoic acid

Base Information

Chemical Name:6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoic acid
CAS No.:1286178-57-1
Molecular Formula:C₂₅H₂₇NO₈S
Molecular Weight:501.557
Hs Code.:

Synonyms:6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoic acid

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Chemical Property of 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoic acid

Chemical Property:

Purity/Quality:

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Technology Process of 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoic acid

There total 9 articles about 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1286178-63-9
ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate

: 1286178-57-1
6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoic acid

Guidance literature:: With lithium hydroxide monohydrate; In 1,4-dioxane; water; at 20 - 100 ℃;

Reference yield:

: 1286179-51-8
ethyl 6-(benzenesulphonylmethyl)-3-bromo-2-methoxybenzoate

: 1286178-57-1
6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: boron tribromide / dichloromethane / -70 - 20 °C

2: potassium fluoride monohydrate; sodium bromide / tetrakis(triphenylphosphine) palladium(0) / α,α,α-trifluorotoluene / 0.5 h / 175 °C / Microwave

3: caesium carbonate / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

4: lithium hydroxide monohydrate / 1,4-dioxane; water / 20 - 100 °C

With lithium hydroxide monohydrate; potassium fluoride monohydrate; boron tribromide; caesium carbonate; sodium bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; α,α,α-trifluorotoluene; water; N,N-dimethyl-formamide;

Reference yield:

: 1286179-34-7
ethyl 6-(benzenesulphonylmethyl)-3-bromo-2-hydroxybenzoate

: 1286178-57-1
6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium fluoride monohydrate; sodium bromide / tetrakis(triphenylphosphine) palladium(0) / α,α,α-trifluorotoluene / 0.5 h / 175 °C / Microwave

2: caesium carbonate / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

3: lithium hydroxide monohydrate / 1,4-dioxane; water / 20 - 100 °C

With lithium hydroxide monohydrate; potassium fluoride monohydrate; caesium carbonate; sodium bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; α,α,α-trifluorotoluene; water; N,N-dimethyl-formamide;