ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate

Base Information

Chemical Name:ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate
CAS No.:1286178-63-9
Molecular Formula:C₂₇H₃₁NO₈S
Molecular Weight:529.611
Hs Code.:

Synonyms:ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate

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Chemical Property of ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate

Chemical Property:

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Technology Process of ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate

There total 8 articles about ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1286179-06-3
ethyl 6-(benzenesulphonylmethyl)-3-(furan-3-yl)-2-hydroxybenzoate

: 39684-80-5
2-(tert-butoxycarbonylamino)ethyl bromide

: 1286178-63-9
ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;

Reference yield:

: 1286179-51-8
ethyl 6-(benzenesulphonylmethyl)-3-bromo-2-methoxybenzoate

: 1286178-63-9
ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: boron tribromide / dichloromethane / -70 - 20 °C

2: potassium fluoride monohydrate; sodium bromide / tetrakis(triphenylphosphine) palladium(0) / α,α,α-trifluorotoluene / 0.5 h / 175 °C / Microwave

3: caesium carbonate / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

With potassium fluoride monohydrate; boron tribromide; caesium carbonate; sodium bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; α,α,α-trifluorotoluene; N,N-dimethyl-formamide;

Reference yield:

: 1286179-34-7
ethyl 6-(benzenesulphonylmethyl)-3-bromo-2-hydroxybenzoate

: 1286178-63-9
ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium fluoride monohydrate; sodium bromide / tetrakis(triphenylphosphine) palladium(0) / α,α,α-trifluorotoluene / 0.5 h / 175 °C / Microwave

2: caesium carbonate / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

With potassium fluoride monohydrate; caesium carbonate; sodium bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In α,α,α-trifluorotoluene; N,N-dimethyl-formamide;