Carbazol-9-yl-acetic acid [1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

Base Information

Chemical Name:Carbazol-9-yl-acetic acid [1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazide
CAS No.:202655-33-2
Molecular Formula:C₂₁H₁₆ClN₃O
Molecular Weight:361.831
Hs Code.:

Synonyms:Carbazol-9-yl-acetic acid [1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

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Chemical Property of Carbazol-9-yl-acetic acid [1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

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Technology Process of Carbazol-9-yl-acetic acid [1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

There total 3 articles about Carbazol-9-yl-acetic acid [1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 202655-30-9
(N⁹-carbazolylacetyl)hydrazine

: 104-88-1
4-chlorobenzaldehyde

: 202655-33-2
Carbazol-9-yl-acetic acid [1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: With acetic acid; In chloroform; Heating;

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 202655-33-2
Carbazol-9-yl-acetic acid [1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / K₂CO₃ / acetone / 13 h / Heating

2: 82 percent / NH₂NH₂*H₂O / dioxane / 8 h / Heating

3: 80 percent / glacial acetic acid / CHCl₃ / Heating

With potassium carbonate; hydrazine hydrate; acetic acid; In 1,4-dioxane; chloroform; acetone;

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 202655-33-2
Carbazol-9-yl-acetic acid [1-(4-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / K₂CO₃ / acetone / 12 h / Heating

2: 82 percent / hydrazine hydrate / dioxane / 18 h / Heating

3: 80 percent / gl. acetic acid / CHCl₃ / Heating

With potassium carbonate; hydrazine hydrate; acetic acid; In 1,4-dioxane; chloroform; acetone; 1: Alkylation / 2: hydrazinolysis / 3: Condensation;