[Co(bis[2-hydroxy-4-(4-vinylbenzylmethoxy)benzaldehyde]ethylenediimine)(4-(dimethylamino)pyridine)2][PF₆]

Base Information

• Chemical Name: [Co(bis[2-hydroxy-4-(4-vinylbenzylmethoxy)benzaldehyde]ethylenediimine)(4-(dimethylamino)pyridine)2][PF₆]
• CAS No.: 284034-50-0
• Molecular Formula: C₄₈H₅₀CoN₆O₄*F₆P
• Molecular Weight: 978.92

Synonyms:[Co(bis[2-hydroxy-4-(4-vinylbenzylmethoxy)benzaldehyde]ethylenediimine)(4-(dimethylamino)pyridine)2][PF₆]

Chemical Property of [Co(bis[2-hydroxy-4-(4-vinylbenzylmethoxy)benzaldehyde]ethylenediimine)(4-(dimethylamino)pyridine)2][PF₆]

Chemical Property:

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Technology Process of [Co(bis[2-hydroxy-4-(4-vinylbenzylmethoxy)benzaldehyde]ethylenediimine)(4-(dimethylamino)pyridine)2][PF₆]

There total 1 articles about [Co(bis[2-hydroxy-4-(4-vinylbenzylmethoxy)benzaldehyde]ethylenediimine)(4-(dimethylamino)pyridine)2][PF₆] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

dmap (1122-58-3) + ferrocenium hexafluorophosphate + cobalt(II) acetate (71-48-7,917-69-1,5931-89-5,55881-15-7,68931-68-0,68931-69-1,93029-27-7) + bis[2-hydroxy-4-(4-vinylbenzylmethoxy)benzaldehyde]ethylenediimine → [Co(bis[2-hydroxy-4-(4-vinylbenzylmethoxy)benzaldehyde]ethylenediimine)(4-(dimethylamino)pyridine)2][PF6] (284034-50-0)

Guidance literature:

In methanol; 1,2-dichloro-ethane; MeOH soln. of Co(OAc)2 (1.86 mmol) was added with stirring to a suspn. of a ligand in a 1,2-dichloroethane; 4-(dimethylamino)pyridine (3.72 mmol) in MeOH and ferrocenium hexafluorophosphate (1.86 mmol) in MeOH were added to the mixt.; under Ar; the react. was stirred for 12 h; volatile compds. were removed under reduced pressure to yield a brown solid; the solid was filtered and washed with Et2O, a 3:1 diethyl ether:MeOH soln., and Et2O; the solid was driedunder vac. overnight; elem. anal.;

DOI:10.1021/ja003282b

upstream raw materials:

dmap

cobalt(II) acetate

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