[(2S,3S,4R)-5-Iodo-2,4-dimethyl-3-(2-methyl-propenyloxy)-pentyloxymethyl]-benzene

Base Information

Chemical Name:[(2S,3S,4R)-5-Iodo-2,4-dimethyl-3-(2-methyl-propenyloxy)-pentyloxymethyl]-benzene
CAS No.:683278-53-7
Molecular Formula:C₁₈H₂₇IO₂
Molecular Weight:402.316
Hs Code.:

Synonyms:[(2S,3S,4R)-5-Iodo-2,4-dimethyl-3-(2-methyl-propenyloxy)-pentyloxymethyl]-benzene

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Chemical Property of [(2S,3S,4R)-5-Iodo-2,4-dimethyl-3-(2-methyl-propenyloxy)-pentyloxymethyl]-benzene

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Technology Process of [(2S,3S,4R)-5-Iodo-2,4-dimethyl-3-(2-methyl-propenyloxy)-pentyloxymethyl]-benzene

There total 10 articles about [(2S,3S,4R)-5-Iodo-2,4-dimethyl-3-(2-methyl-propenyloxy)-pentyloxymethyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 41632-89-7
isobutyraldehyde dimethyl acetal

: (2S,3S,4R)-1-Benzyloxy-5-iodo-2,4-dimethyl-pentan-3-ol

: 683278-53-7
[(2S,3S,4R)-5-Iodo-2,4-dimethyl-3-(2-methyl-propenyloxy)-pentyloxymethyl]-benzene

Guidance literature:: With pyridinium p-toluenesulfonate; In benzene; for 18h; Heating;
DOI:10.1021/jo035310p

Reference yield:

: 108393-28-8
(2S,3R,4S)-5-benzyloxy-2,3-dimethylpentane-1,4-diol

: 683278-53-7
[(2S,3S,4R)-5-Iodo-2,4-dimethyl-3-(2-methyl-propenyloxy)-pentyloxymethyl]-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / pyridine / CH₂Cl₂ / 24 h / 0 °C

2: 69 percent / NaI / acetone / 24 h / 85 °C

3: 55 percent / PPTS / benzene / 18 h / Heating

With pyridine; pyridinium p-toluenesulfonate; sodium iodide; In dichloromethane; acetone; benzene;
DOI:10.1021/jo035310p

Reference yield:

: 100-39-0
benzyl bromide

: 683278-53-7
[(2S,3S,4R)-5-Iodo-2,4-dimethyl-3-(2-methyl-propenyloxy)-pentyloxymethyl]-benzene

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / NaH / dimethylformamide / 24 h / 0 °C

2: 96 percent / TsOH / methanol / 24 h / 20 °C

3: 81 percent / pyridine / CH₂Cl₂ / 24 h / 0 °C

4: 69 percent / NaI / acetone / 24 h / 85 °C

5: 55 percent / PPTS / benzene / 18 h / Heating

With pyridine; pyridinium p-toluenesulfonate; sodium hydride; toluene-4-sulfonic acid; sodium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/jo035310p